Principles of Thermal Analysis and Calorimetry 1st Edition by Peter Haines ISBN 9780854046102 085404610

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Product details: 

ISBN 10: 085404610

ISBN 13: :  9780854046102

Author:  Peter Haines 

This book is up-to-date, wide-ranging and practical and will be an important source of information for many levels of readership in a variety of areas.

Table of contents: 

Chapter 1
Introduction
P. J. Haines

Materials, Heat and Changes
Definitions of Thermal and Calorimetric Methods
The Family of Thermal Methods
Instrumentation for Thermal Analysis and Calorimetry
The Reasons for Using Thermal and Calorimetric Methods
The Need for Proper Practice
Further Reading

Chapter 2
Thermogravimetry and Derivative Thermogravimetry
G. R. Heal
Introduction and Definitions
Instrumentation
Balance
Furnace
Atmosphere Control
Crucibles
Thermocouples
Temperature Control
Data Collection
Isothermal Experiments
Calibration for Mass and Temperature
Effect of Experimental Variables
Reporting Thermogravimetry Results
A. Properties of the Sample
B. Experimental Conditions

C. Data Acquisition and Manipulation Methods
D. Results
A Typical Thermogravimetric Experiment
Preliminary Steps
Crucible Treatment
Zero Setting
Adding the Sample
Starting the Run
Ending the Run
Example Experiment
Results
Applications
Oxysalt Decomposition
Polymer Stability and Charcoal Production
Metal Oxidation
Compositional Analysis
Glass-making Reactions
Kinetics of Solid-state Reactions
Ancillary Techniques
Residue Analysis
Other Temperature Regimes

Chapter 3: Differential Thermal Analysis and Differential Scanning Calorimetry

Introduction
Definitions and Nomenclature
Applications
Theoretical Considerations
Instrumentation
Specification
Temperature Sensors
Crucibles
Temperature and Atmosphere Control
Cooling Systems and Accessories
Calvet-type Equipment
Experimental Considerations
Variables
Do’s and Do not’s
Reference
Calibration
Preliminaries
Temperature Calibration
Energy Calibration
Measurements
Measurement of Heat Capacity
Measurement of Energy
Measurement of Purity
Kinetics
Final Thoughts on Measurement
Further Reading
References
2. Chapter 4: Thermomechanical, Dynamic Mechanical and Dielectric Methods

Introduction and Principles
Thermomechanical Analysis and Thermodilatometry
Dynamic Mechanical Analysis
Dielectric Techniques
Instrumentation
Thermomechanical Analysis
Dynamic Mechanical Analysis
Dielectric Techniques
Typical Experiments
Thermomechanical Analysis
Dynamic Mechanical Analysis
Dielectric Techniques
Applications
Thermomechanical Analysis
Dynamic Mechanical Analysis
Dielectric Thermal Analysis
Modulated Temperature Thermomechanical and Dielectric
3. A Typical Thermogravimetric Experiment

Preliminary Steps
Crucible Treatment
Zero Setting
Adding the Sample
Starting the Run
Ending the Run
Example Experiment
Results
4. Applications

Oxysalt Decomposition
Polymer Stability and Charcoal Production
Metal Oxidation
Compositional Analysis
Glass-making Reactions
Kinetics of Solid-state Reactions
5. Ancillary Techniques

Residue Analysis
Other Temperature Regimes

Chapter 5
Calorimetry
R. J. Willson

Introduction
Definition of Calorimetry
Thermochemistry and Thermodynamics
The First Law of Thermodynamics
The Second Law of Thermodynamics
The Third Law of Thermodynamics
Calorimeters
Classification of Calorimeters
Calibration
Instrumentation: Calorimeters for Special Purposes
Solution Calorimeters
Combustion Calorimeters
Reaction Hazard Calorimeters
Isothermal Calorimeters
Applications of Isothermal Calorimetry
Calorimetric Information
The Calorimetric Signal
Reaction Mechanism
Kinetic Information
Examples of Calorimetric Applications
Chemical Reactions
Physical Changes
Summary
Acknowledgements
References
Chapter 6
Simultaneous Thermal Analysis Techniques
S. B. Warrington

Introduction: The Rationale behind the Simultaneous Approach
Simultaneous Thermogravimetry–Differential Thermal Analysis (TG-DTA)
Instrumentation
Applications of TG-DTA
Simultaneous Thermogravimetry–Differential Scanning Calorimetry (TG-DSC)
Instrumentation
Applications of TG-DSC
Evolved Gas Analysis (EGA)
Introduction
Instrumentation for EGA
Applications of EGA
Less Common Techniques
Optical Techniques
Spectroscopic Techniques
X-Ray Techniques
DTA–Rheometry
Micro-thermal Analysis (μ-TA)
Summary
References

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Peter Haines,Thermal Analysis,Calorimetry