Polymer Morphology Principles Characterization and Processing 1st Edition by Qipeng Guo ISBN 1118452151 9781118452158

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ISBN 10: 1118452151 
ISBN 13: 9781118452158
Author:  Qipeng Guo

With a focus on structure-property relationships, this book describes how polymer morphology affects properties and how scientists can modify them. The book covers structure development, theory, simulation, and processing; and discusses a broad range of techniques and methods. • Provides an up-to-date, comprehensive introduction to the principles and practices of polymer morphology • Illustrates major structure types, such as semicrystalline morphology, surface-induced polymer crystallization, phase separation, self-assembly, deformation, and surface topography • Covers a variety of polymers, such as homopolymers, block copolymers, polymer thin films, polymer blends, and polymer nanocomposites • Discusses a broad range of advanced and novel techniques and methods, like x-ray diffraction, thermal analysis, and electron microscopy and their applications in the morphology of polymer materials

Polymer Morphology Principles Characterization and Processing 1st Table of contents:

Part I: Principles and Methods of Characterization
Chapter 1: Overview and Prospects of Polymer Morphology
1.1 Introductory Remarks
1.2 Experimental Avenues of Morphological Research
1.3 Modeling and Simulation
1.4 Wishful Thinking
1.5 Summary
References
Chapter 2: X-ray Diffraction from Polymers
2.1 Introduction
2.2 Basic Principles
2.3 Instrumentation
2.4 Structure Determination
2.5 Phase Analysis
2.6 Crystallite Size and Disorder
2.7 Orientation Analysis
2.8 Small-Angle Scattering
2.9 Specialized Measurements
2.10 Summary
References
Chapter 3: Electron Microscopy of Polymers
3.1 Introduction
3.2 Microscopic Techniques
3.3 Sample Preparation
3.4 In situ Microscopy
References
Chapter 4: Characterization of Polymer Morphology by Scattering Techniques
4.1 Introduction
4.2 A Short Theoretical Presentation
4.3 Experimental Aspects
4.4 Typical Results
4.5 Concluding Remarks
References
Chapter 5: Differential Scanning Calorimetry of Polymers
5.1 Introduction to Differential Scanning Calorimetry. Basic Principles and Types of DSC Equipment
5.2 Detection of First-Order and Second-Order Transitions by DSC. Applications of Standard DSC Experiments to the Determination of the Glass Transition Temperature and the Melting Temperature of Polymeric Materials
5.3 Self-Nucleation
5.4 Thermal Fractionation
5.5 Multiphasic Materials: Polymer Blends and Block Copolymers. Fractionated Crystallization and Confinement Effects
5.6 Self-Nucleation and the Efficiency Scale to Evaluate Nucleation Power
5.7 Determination of Overall Isothermal Crystallization by DSC
5.8 Conclusions
Acknowledgment
References
Chapter 6: Imaging Polymer Morphology using Atomic Force Microscopy
6.1 Introduction
6.2 Fundamental AFM Techniques
6.3 Imaging of Polymer Morphology
6.4 Property Mapping
References
Chapter 7: FTIR Imaging of Polymeric Materials
7.1 Introduction
7.2 Principles of FTIR Imaging
7.3 Sampling Methods
7.4 Spatial Resolution
7.5 Recent Applications
7.6 Conclusions
References
Chapter 8: NMR Analysis of Morphology and Structure of Polymers
8.1 Introduction
8.2 Basic Concepts in NMR
8.3 Morphology and Relaxation Behavior of Polyethylene
8.4 Morphology and Structure of the Nascent Powders
8.5 Kinetics of Dynamic Process of Polymers
8.6 Conclusions
References
Part II: Morphology, Properties, and Processing
Chapter 9: Small-Angle X-ray Scattering for Morphological Analysis of Semicrystalline Polymers
9.1 Introduction
9.2 Small-angle X-ray Scattering
9.3 Concluding Remarks
Appendix: Calculation of the Model Function K”sim(s)
References
Chapter 10: Crystalline Morphology of Homopolymers and Block Copolymers
10.1 Introduction
10.2 Crystalline Morphology of Homopolymers
10.3 Crystalline Morphology of Block Copolymers
10.4 Concluding Remarks
References
Chapter 11: Isothermal Crystallization Kinetics of Polymers
11.1 Introduction
11.2 Crystallization Process
11.3 Crystallization Kinetics
11.4 Isothermal Crystallization Kinetics – Morphology Relationship
11.5 Conclusions
Acknowledgments
References
Chapter 12: Surface-induced Polymer Crystallization
12.1 Introduction
12.2 Influence of Foreign Surface on the Crystallization Kinetics of Polymers
12.3 Influence of Foreign Surface on the Crystal Structure and Morphology of Polymers
12.4 Bulk Crystallization of Polymers in Contact with a Foreign Surface
12.5 Summary
References
Chapter 13: Thermodynamics and Kinetics of Polymer Crystallization
13.1 Introduction
13.2 Thermodynamics of Polymer Crystallization
13.3 Crystal Nucleation
13.4 Crystal Growth
13.5 Crystal Annealing
13.6 Summary
References
Chapter 14: Self-Assembly and Morphology in Block Copolymer Systems with Specific Interactions
14.1 Introduction
14.2 Block Copolymer Systems with Hydrogen Bonding Interaction in Solid State
14.3 Block Copolymer Systems with Hydrogen-Bonding Interaction in Solution
14.4 Block Copolymer Systems with Ionic Interaction
14.5 Block Copolymer Blends via Metal–Ligand Coordination Bonds
14.6 Concluding Remarks
References
Chapter 15: Dynamics Simulations of Microphase Separation in Block Copolymers
15.1 Introduction
15.2 Polymer Model and Simulation Algorithm
15.3 Dynamics of Self-Assembly of Block Copolymers
15.4 Outlook
References
Chapter 16: Morphology Control of Polymer thin Films
16.1 Wetting
16.2 Thin Film of Polymer Blend
16.3 The Introduction of Polymer Blend Film in Solar Cells
16.4 Summary and Outlook
References
Chapter 17: Polymer Surface Topography and Nanomechanical Mapping
17.1 Introduction
17.2 Contact Mechanics
17.3 Application of Contact Mechanics to Experimental Data
17.4 Application Examples
17.5 Conclusion
References
Chapter 18: Polymer Morphology and Deformation Behavior
18.1 Introduction
18.2 Deformation Behavior of Amorphous Polymers
18.3 Deformation Behavior of Semicrystalline Polymers
18.4 Deformation Behavior of Block Copolymers
18.5 Conclusions and Outlook
References
Chapter 19: Morphology Development in Immiscible Polymer Blends
19.1 Introduction
19.2 Morphology Development in Bulk Flow
19.3 Recent Advances in Polymer Blends
19.4 Conclusions
Acknowledgments
References
Chapter 20: Processing, Structure, and Morphology in Polymer Nanocomposites
20.1 Overview
20.2 Nanoparticles with One Dimension Less Than 100 nm (Layered Silicates)
20.3 Nanoparticles with Two Dimensions Less Than 100 nm (Carbon Nanotubes)
20.4 Nanoparticles with Three Dimensions Less Than 100 nm (Metal, Metal Oxide)
20.5 Preparative Methods
20.6 Structure and Morphology of Polymer Nanocomposites
20.7 Concluding Remarks
References
Chapter 21: Morphology and Gas Barrier Properties of Polymer Nanocomposites
21.1 Introduction
21.2 Structure of Layered Silicates
21.3 Morphologies of Polymer-Layered Silicate Composites
21.4 Nanocomposite Preparation Methods
21.5 Challenges of Thermal Degradation in Melt Intercalation
21.6 Methods for Improving Gas Barrier Properties of Polymers
21.7 Polyamide Nanocomposites
21.8 Polyolefin Nanocomposites
21.9 Pet Nanocomposites
21.10 Polylactide Nanocomposites
21.11 Conclusions and Perspectives
References
Chapter 22: Features on the Development and Stability of Phase Morphology in Complex Multicomponent Polymeric Systems: Main Focus on Processing Aspects
22.1 Introduction
22.2 Phase Morphology Development in Polymer Blends
22.3 Melt Processing of Polymer Blends
22.4 Chemistry Involved in Polymer Blends

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Tags: Qipeng Guo, Polymer, Morphology