(Ebook PDF) Fundamentals of Fourier Transform Infrared Spectroscopy Second Edition by Brian Smith-Ebook PDF Instant Download/Delivery:9781040068366, 1040068367
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ISBN 10:1040068367
ISBN 13:9781040068366
Author: Brian C. Smith
Reflecting the myriad changes and advancements in the technologies involved in FTIR, particularly the development of diamond ATRs, this second edition of Fundamentals of Fourier Transform Infrared Spectroscopy has been extensively rewritten and expanded to include new topics and figures as well as updates of existing chapters. Designed for those ne
Table of Contents:
- Chapter 1 Introduction To Infrared Spectroscopy
- I. Terms And Definitions
- II. The Properties Of Light
- III. What Is An Infrared Spectrum?
- IV. What Are Infrared Spectra Used For?
- V. The Advantages And Disadvantages Of Infrared Spectroscopy
- VI. The Advantages And Disadvantages Of Ftir
- A. The Advantages Of Ftirs
- B. The Disadvantage Of Ftir
- VII. Ftir: The Rest Of The Story
- References
- Chapter 2 How An Ftir Works
- I. Interferometers And Interferograms
- A. How Many Scans Should Be Used?
- II. How An Interferogram Becomes A Spectrum
- A. Scanning Advice
- III. Instrumental Resolution
- A. What Determines Resolution In An Ftir Scan?
- B. What Resolution Should Be Used?
- IV. Ftir Trading Rules
- V. Ftir Hardware
- A. Interferometers
- B. Infrared Sources
- C. Beamsplitters
- D. Infrared Detectors
- E. The Laser
- VI. Testing Instrument Quality And Troubleshooting
- References
- Chapter 3 Proper Use Of Spectral Processing
- I. The Rules Of Spectral Processing
- II. Spectral Subtraction
- A. Subtraction Artifacts
- III. Baseline Correction
- IV. Smoothing
- V. Spectral Derivatives
- VI. Deconvolution
- A. Guidance, Precautions, And Limitations
- VII. Spectral Library Searching
- A. The Search Process
- B. Interpreting Library Search Results
- VIII. Analysis Of Mixtures: Subtract And Search Again
- References
- Chapter 4 Preparing Samples Properly
- I. Transmission Sampling Overview
- A. Windows, Cells, And Materials For Transmission Analysis
- II. Transmission Analysis Of Solids And Powders
- A. Kbr Pellets
- 1. Mechanical Grinding
- 2. Advantages And Disadvantages Of Kbr Pellets
- B. Mulls
- 1. The Split Mull Method
- III. Transmission Analysis Of Polymers
- A. The Cast Film Method
- B. The Heat And Pressure Method
- IV. Transmission Analysis Of Liquids
- A. Capillary Thin Films
- B. Sealed Liquid Cells
- V. Transmission Analysis Of Gases And Vapors
- VI. Reflectance Analysis
- A. Different Types Of Reflectance
- B. Advantages And Disadvantages Of Reflectance Sampling
- VII. Specular Reflectance
- VIII. Diffuse Reflectance (Drifts)
- A. Abrasive Sampling
- IX. Attenuated Total Reflectance (Atr)
- A. Depth Of Penetration
- X. Applications Of Atr
- A. Liquids
- B. Semi-Solids
- C. Polymers
- D. Powders
- XI. Atr: Advantages And Disadvantages
- XII. Ftir Sample Preparation: Overview And Recommendations
- References
- Chapter 5 Quantitative Infrared Spectroscopy
- I. Terms And Definitions
- II. Beer’S Law
- III. Calibration And Prediction With Beer’S Law A. Calibration
- B. Prediction
- C. An Experimental Protocol For Single Component Analyses
- 1. Analyzing For A Single Analyte
- IV. Measuring Absorbances Properly
- A. Peak Areas Versus Peak Heights
- B. Dealing With Overlapped Peaks
- V. Avoiding Experimental Errors
- Bibliography
- References
- Chapter 6 Infrared Microscopy
- I. Hyphenated Infrared Techniques
- II. Infrared Microscopy Instrumentation
- III. Sample Preparation
- IV. Applications
- V. Infrared Mapping And Imaging
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