Crystal Structure Analysis A Primer 3rd Edition by Glusker, Kenneth Trueblood ISBN 978-0199576357 0199576351

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Product details: 

ISBN 10: 0199576351

ISBN 13: 978-0199576357

Author: Glusker J.P., Kenneth N. Trueblood

Crystal Structure Analysis, Third Edition, explains how and why the detailed three-dimensional architecture of molecules can be determined by an analysis of the diffraction patterns obtained when X-rays or neutrons are scattered by the atoms in single crystals. Part 1 covers the nature of the crystalline state, diffraction in general, and diffraction by crystals, and also looks briefly at experimental procedures. Part II examines the problem of converting the experimentally obtained data into a model of the atomic arrangement that scattered these beams. Part III discusses techniques for refining the approximate structure to the degree warranted by the experimental data. It also describes the many types of information that can be obtained by modern crystal structure analysis. The text is enhanced by numerous illustrations, a detailed glossary, and several appendices that cover mathematical details.

Table of contents: 

I: CRYSTALS AND DIFFRACTION
1. Introduction
2. Crystals
3. Diffraction
4. Experimental Measurements
II: DIFFRACTION PATTERNS AND THEIR ANALYSIS
5. The Diffraction Pattern Obtained
6. The Phase Problem
7. Symmetry and Space Groups
8. The Derivation of Trial Structures: I. Analytical Methods of Direct Phase Determination
9. The Derivation of Trial Structures: II. Patterson, Heavy Atom, and Isomorphous Replacement Methods
10. Anomalous Dispersion and Absolute Configuration
III: STRUCTURE REFINEMENT AND STRUCTURAL INFORMATION
11. Refinement of the Trial Structure
12. Structural Parameters: Analysis of Results
13. Micro- and Noncrystalline Structures
14. Outline of a Crystal Structure Determination

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Tags: Glusker, Kenneth Trueblood, Crystal Structure, Analysis A Primer