Capillary Electrochromatography 1st Edition by Zdeněk Deyl, Frantiaek `Vec ISBN 9780444504326, 044450432X
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ISBN 10: 044450432X
ISBN 13: 9780444504326
Author: Zdeněk Deyl, Frantiaek `Vec
Academic material: Capillary Electrochromatography 1st Edition Zdeněk Deyl And Frantiaek `Vec (Eds.)Available for instant access. A structured learning tool offering deep insights, comprehensive explanations, and high-level academic value.
Table of contents:
Chapter 1
Migration of Charged Sample Components and Electroosmotic Flow in Packed Capillary Columns
Anurag S. Rathore and Csaba Horváth
1.1 Introduction.
1.2 Flow of ions in open tubes
1.3 Electroosmotic flow in open tubes
1.4 Flow of ions in packed columns
1.5 Electroosmotic flow through packed columns
1.6 Conclusions.
1.7 Symbols and abbreviations
1.8 References
Instrumentation for Capillary Electrochromatography
Chapter 2
Gerard P. Rozing. Anna Dermaux and Pat Sandra
2.1 Introduction.
2.2 Instrumentation requirements
2.3 Gradient-CEC instrumentation
2.4 Detection
2.5 Summary and conclusion.
2.6 References
Modes of CEC Separation
Chapter 3
Christopher M. Johnson, Alan P. McKeown and Melvin R. Euerby
3.1 Introduction.
3.2 Definitions
3.3 Unmodified packings.
3.4 Modified packings
3.5 Chiral stationary phases
3.6 CEC Gel
3.7 Monoliths
3.8 Size exclusion CEC
3.9 Gradient CEC.
3.10 Selectivity compared with I.C
3.11 Guidelines for the analysis of acidic basic and neutral compounds
3.12 Conclusions.
3.13 Abbreviations.
3.14 References
Chapter 4 Packed Bed Columns
Luis A. Colón, Todd D. Maloney and Adam M. Fermier
4.1 Introduction.
4.2 Column fabrication
4.3 Packing methods
4.4 Comparison of packing procedures
4.5 Conclusions
4.6 Acknowledgement
4.7 Abbreviations .
4.8 References
Chapter 5
Capillary Electrochromatography on Monolithic Silica Columns
Nobuo Tanaka and Hiroshi Kobayashi
5.1 Introduction
5.2 Monolithic silica columns
5.3 Preparation procedure of silica monoliths from silane monomers
5.4 Structural properties of monolithic silica columns prepared in a capillary
5.5 Performance of monolithic silica columns in CEC
5.6 References
Chapter 6
Capillary Column Technology: Continuous Polymer Monoliths
František Švec
6.1 Introduction.
6.2 Replaceable polymeric stationary phases.
6.3 Polymer gels
6.4 Highly crosslinked acrylamide-based monoliths
6.5 Imprinted enantioselective monoliths
6.6 Polystyrene-based monoliths……
6.7 Methacrylate ester-based monolithic columns
6.8 Assessment of porous structure.
6.9 Effects of properties on the separation ability
6.10 Other applications of porous polymer monoliths in CEC column technology
6.11 Acknowledgment
6.12 References
Chapter 7
Open Tubular Approaches to Capillary Electrochromatography
Joseph J. band Maria T. Matyska
7.1 Introduction.
7.2 Chemical etching process
7.3 Chemical modification process…
7.4 Characterization of etched, chemically modified capillaries
7.5 Applications of OTCEC
7.6 Conclusions.
7.7 Abbreviations.
7.8 References
Chapter 8
Hyphenation of Capillary Electrochromatography and Mass Spectrometry: Instrumental Aspects, Separation Systems,
and Applications Christian G. Huber and Georg Hölzi
8.1 Introduction.
8.2 Instrumentation and technology for coupling of CEC and MS
8.3 Stationary phase-mobile phase systems used for CEC-MS
8.4 Optimization of electrochromatographic and mass spectrometric conditions
8.5 Examples of application
8.6 Acknowledgments
8.7 References
Chapter 9
Pressure Supported CEC: a High-Efficiency Technique
for Enantiomer Separation
Dorothee Wistuba and Volker Schurig
9.1 Introduction
9.2 Techniques of pressurizing
9.3 Theory
9.4 Instrumentation
9.5 Applications
9.6 Advantages and disadvantages of pressurized CEC
9.7 Conclusion and future trends
9.8 Abbreviations.
9.9 Acknowledgement
9.10 References
Chapter 10 Applications.
Zdeněk Deyl and Ivan Mikšik
10.1 Introduction.
10.2 Preconcentration procedures
10.3 Hydrocarbons.
10.4 Ketones.
10.5 Carbohydrates
10.6 Fatty acids
10.7 Triglycerides
10.8 Steroids
10.9 Amino acids
10.10 Peptides
10.11 Nucleic acids constituents
10.12 Drugs
10.13 Antibiotics
10.14 Pesticides
10.15 Available applications (summarizing Table)
10.16 References
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