Chiral Separations by Liquid Chromatography Theory and Applications 1st Edition by Hassan Aboul Enein, Imran Ali ISBN 978-0824740146 0824740149

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Product details: 

ISBN 10:  0824740149

ISBN 13: 978-0824740146

Author: Hassan Y. Aboul-Enein,  Imran Ali 

Unique in its systematic and detailed description of the various types, structures, and properties of chiral stationary phases (CSPs) and their preparation, application, and future scope, this volume highlights an assortment of liquid chromatographic approaches, including sub- and super-critical fluid chromatography, capillary electrochromatography, and thin layer chromatography. Readers will find: viable optimization techniques for enantiomeric resolution on various types of CSPs and new strategies in liquid chromatography and related technologies of chiral separations. It is a valuable resource filled with 1200 of the most recent and relevant literature citations.

Table of contents: 

1 Introduction

1.1 Chirality and Its Occurrence

1.2 Chemical Evolution of Chirality

1.3 Chirality in Molecules

1.4 Chirality and Its Consequences in Biological Systems

1.5 Chirality and Drug Development

1.6 Chiral Drugs and Their Economic Status

1.7 Chirality and Its Consequence in the Environment

1.8 Resolution of Stereoisomers

1.9 Detection in Liquid Chromatography

1.10 Chiral Recognition Mechanisms

2 Polysaccharide-Based Chiral Stationary Phases

2.1 Polysaccharide Derivatives

2.2 Spectroscopic Studies

2.3 Preparation and Commercialization

2.4 Selectivities

2.5 Applications

2.6 Optimization of HPLC Conditions

2.7 Chiral Recognition Mechanisms

2.8 Applications in Sub- and Supercritical Fluid Chromatography

2.9 Applications in Capillary Electrochromatography

2.10 Applications in Thin-Layer Chromatography

2.11 Conclusion

3 Cyclodextrin-Based Chiral Stationary Phases

3.1 Structures and Properties

3.2 Preparation and Commercialization

3.3 Applications

3.4 Optimization of HPLC Conditions

3.5 Chiral Recognition Mechanism

3.6 Applications in Sub- and Supercritical Fluid Chromatography

3.7 Applications in Capillary Electrochromatography

3.8 Conclusion

4 Macrocyclic Glycopeptide Antibiotics-Based Chiral Stationary Phases

4.1 Structures and Properties

4.2 Preparation and Commercialization

4.3 Applications

4.4 Optimization of HPLC Conditions

4.5 Chiral Recognition Mechanism

4.6 Miscellaneous Applications

4.7 Conclusion

5 Pirkle-Type and Related Chiral Stationary Phases

5.1 Structures and Properties

5.2 Preparation and Commercialization

5.3 Applications

5.4 Optimization of High-Performance Liquid Chromatographic Conditions

5.5 Chiral Recognition Mechanism

5.6 Applications in Sub- and Supercritical Fluid Chromatography

5.7 Miscellaneous Applications

5.8 Conclusion

6 Protein-Based Chiral Stationary Phases

6.1 Structures and Properties

6.2 Preparation and Commercialization

6.3 Applications

6.4 Optimization of HPLC Conditions

6.5 Chiral Recognition Mechanism

6.6 Miscellaneous Applications

6.7 Conclusion

7 Ligand Exchange-Based Chiral Stationary Phases

7.1 Structures and Properties

7.2 Preparation and Commercialization

7.3 Applications

7.4 Optimization of High-Performance Liquid Chromatographic Conditions

7.5 Chiral Recognition Mechanism

7.6 Miscellaneous Applications

7.7 Conclusion

8 Crown Ether-Based Chiral Stationary Phases

8.1 Structures and Properties

8.2 Preparation and Commercialization

8.3 Applications

8.4 Optimization of High-Performance Liquid Chromatographic Conditions

8.5 Chiral Recognition Mechanism

8.6 Miscellaneous Applications

8.7 Conclusion

9 Miscellaneous Types of Chiral Stationary Phase

9.1 Alkaloid-Based CSPS

9.2 Amide- and Amine-Based CSPs

9.3 Acid-Based CSPs

9.4 Synthetic Polymer-Based CSPS

9.5 Molecularly Imprinted CSPS

9.6 Miscellaneous CSP in SFC

9.7 Miscellaneous CSP in CEC

9.8 Miscellaneous CSP in TLC

9.9 Chiral Recognition Mechanisms

9.10 Conclusion

10 Enantiomeric Separation by the Chiral Mobile Phase Additives

10.1 Cyclodextrin Mobile Phase Additives

10.2 Ligand-Exchanger Mobile Phase Additives

10.3 Protein Mobile Phase Additives

10.4 Macrocyclic Glycopeptide Antibiotic Mobile Phase Additives

10.5 Miscellaneous Chiral Mobile Phase Additives

10.6 Chiral Mobile Phase Additives in SFC and CEC

10.7 Chiral Mobile Phase Additives in TLC

10.8 Chiral Recognition Mechanisms

10.9 Conclusion

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Tags: Hassan Aboul Enein, Imran Ali, Chiral Separations, Liquid Chromatography, Theory and Applications